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Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds

Received: 8 April 2017     Accepted: 22 May 2017     Published: 13 July 2017
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Abstract

Three Dialdehydes were synthesized by the reaction of Salicylaldehyde and many Aliphatic and Aromatic Halides. The optimal condition (Catalysts, Temperature, Time of Reaction and Effect of Solvents) to get a high selective compounds and high yields have been studied. The reactions were followed by using Thin Layer Chromatography (TLC). The synthesized compounds were purified and characterized by means of High Performance Liquid Chromatography (HPLC) and spectroscopy methods: Infrared Spectra (IR), 1 H-NMR, 13C-NMR.

Published in Journal of Biomaterials (Volume 1, Issue 2)
DOI 10.11648/j.jb.20170102.12
Page(s) 34-39
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2017. Published by Science Publishing Group

Keywords

Salicylaldehyde, Heterogeneous Catalysts, Dialdehyde, Aliphatic and Aromatic Halides

References
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    Joumaa Merza, Ali Alasmi. (2017). Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds. Journal of Biomaterials, 1(2), 34-39. https://doi.org/10.11648/j.jb.20170102.12

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    ACS Style

    Joumaa Merza; Ali Alasmi. Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds. J. Biomater. 2017, 1(2), 34-39. doi: 10.11648/j.jb.20170102.12

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    AMA Style

    Joumaa Merza, Ali Alasmi. Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds. J Biomater. 2017;1(2):34-39. doi: 10.11648/j.jb.20170102.12

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  • @article{10.11648/j.jb.20170102.12,
      author = {Joumaa Merza and Ali Alasmi},
      title = {Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds},
      journal = {Journal of Biomaterials},
      volume = {1},
      number = {2},
      pages = {34-39},
      doi = {10.11648/j.jb.20170102.12},
      url = {https://doi.org/10.11648/j.jb.20170102.12},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.jb.20170102.12},
      abstract = {Three Dialdehydes were synthesized by the reaction of Salicylaldehyde and many Aliphatic and Aromatic Halides. The optimal condition (Catalysts, Temperature, Time of Reaction and Effect of Solvents) to get a high selective compounds and high yields have been studied. The reactions were followed by using Thin Layer Chromatography (TLC). The synthesized compounds were purified and characterized by means of High Performance Liquid Chromatography (HPLC) and spectroscopy methods: Infrared Spectra (IR), 1 H-NMR, 13C-NMR.},
     year = {2017}
    }
    

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    T1  - Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds
    AU  - Joumaa Merza
    AU  - Ali Alasmi
    Y1  - 2017/07/13
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    N1  - https://doi.org/10.11648/j.jb.20170102.12
    DO  - 10.11648/j.jb.20170102.12
    T2  - Journal of Biomaterials
    JF  - Journal of Biomaterials
    JO  - Journal of Biomaterials
    SP  - 34
    EP  - 39
    PB  - Science Publishing Group
    SN  - 2640-2629
    UR  - https://doi.org/10.11648/j.jb.20170102.12
    AB  - Three Dialdehydes were synthesized by the reaction of Salicylaldehyde and many Aliphatic and Aromatic Halides. The optimal condition (Catalysts, Temperature, Time of Reaction and Effect of Solvents) to get a high selective compounds and high yields have been studied. The reactions were followed by using Thin Layer Chromatography (TLC). The synthesized compounds were purified and characterized by means of High Performance Liquid Chromatography (HPLC) and spectroscopy methods: Infrared Spectra (IR), 1 H-NMR, 13C-NMR.
    VL  - 1
    IS  - 2
    ER  - 

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Author Information
  • Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria

  • Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria

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